Constant Current Source for Coulometry (Group D) Nick Ben, Louis Muldrow, Yuan Liu, Bastien Levadoux, Nayyara Shaik Mentors: Frank Cardone, Dr. Skip Pomeroy

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Statement of Work (SOW) Our Role: Gather coulometer's data and use a cell phone as the I/O device. (Current and time need to be logged during the analysis). Analog switch replaced by digital switch (Bluetooth enabled) Data communicated from the coulometer to a cell phone Various readings displayed on Mobile Application

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Parts we Received

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Coulometer Device Schematic

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Built Constant Current Source

Analog Switch

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SOW (Main Goals)  Analog Switch in Coulometer replaced by Digital Switch  NPN Transistor

 Data communicated from the coulometer to a cell phone  Arduino Uno Module + BLE Module

 Various readings displayed on Mobile Application  Android App Displays: 1. Interval X Voltage, 2. Interval X Current, 3. Interval X Charge

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SOW Goal 1 Analog Switch Replaced by Digital Switch

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Analog Switch Replaced by Digital Switch

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NPN BJT Transistor Switch Base voltage < 0.6v



BJT Open circuit



No current flow

Base voltage > 0.6v •

Base current above 0



BJT Short circuit



emmiter connected to ground

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BJT Switch On

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BJT Switch Off

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SOW Goal 2 Data Communicated from Coulometer to Cell Phone

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Data Communicated from Coulometer to Cell Phone  Bluetooth Low Energy: - Low cost - Low consumption - Small

- Fast (enough) - Easy to use coupled with a mobile app

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Data Communicated from Coulometer to Cell Phone  Initiate the communication :

 Communicate between devices :

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Data Communicated from Coulometer to Cell Phone

Prepend char X

Extendable

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Data Communicated from Coulometer to Cell Phone Older version of command receiving

single character limit no prepend

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Data Communicated from Coulometer to Cell Phone New version

Loop time controllable

Transmission controllable

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SOW Goal 3 Various Readings Displayed on Mobile Application

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Various Readings Displayed on Mobile Application Main Activity

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Various Readings Displayed on Mobile Main Activity App Bluetooth Connection

V/I Data + Charge

Start/Pause/Save/Reset Buttons

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Various Readings Displayed on Mobile Collecting Data w/ Application (2) Pause/Resume

Collecting Data

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Various Readings Displayed on Mobile Application (3)  Stretch Goal - Saved Data Page

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Various Readings Displayed on Mobile Application (4) Activity Sketches (3rd Screen)

Experiment Details

V/I Data

Charge Data + Buttons

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SOW (Main Goals)  Analog Switch in Coulometer replaced by Digital Switch  NPN Transistor

 Data communicated from the coulometer to a cell phone  Arduino Uno Module + BLE Module

 Various readings displayed on Mobile Application  Android App Displays: 1. Interval X Voltage, 2. Interval X Current, 3. Interval X Charge

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Things to work on...

Digital Switch needs to be implemented...

Test Application (Fix Discrepancy between Multimeter and App)

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Stretch Goals  Improve constant current circuit to make current as a f(time)

 Compute concentration of electrons in the acid

 Display system in a clear case/prototype stage

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Our Stretch Goals Save/Store/View Data, all marked by timestamps Display I, V, Charge when user hits 'Stop'

Display total duration of each test

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Gantt Chart Update

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Sources  Swim, James, Edward Earps, and David Paul. Constant-Current Coulometric Titration of Hydrochloric Acid. Tech. no. 7, Pg 680. Vol. 73. University of Arkansas: Department of Chemistry, July 1996. Print.

 " Coulometric Titration of HCL" Experimental Guidelines - Dr. Skip Pomeroy

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Constant Current Source for Coulometry

Various readings displayed on Mobile Application. Android App Displays: 1. Interval X Voltage, 2. Interval X Current, 3. Interval ... Page 10. BJT Switch On. 10 ...

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